Controlled stepwise synthesis and characterization of a ternary multicomponent crystal with 2-methylresorcinol
- A typical approach of a multicomponent crystal design starts with a retrosynthetic analysis of the target molecule followed by a one-pot reaction of all components. To develop protocols for multicomponent crystal syntheses, controlled stepwise syntheses of a selected crystalline ternary multicomponent system \(\bf 1\) involving 2-methylresorcinol (MRS), tetramethyl-pyrazine (TMP), and 1,2-bis(4-pyridyl)ethane (BPE) are presented. The obtained binary cocrystals \(\bf 2\) (involving MRS and TMP) and \(\bf 3\) (involving MRS and BPE) as well as the final resulting ternary multicomponent system \(\bf 1\) were characterized by X-ray analysis.
Author: | Daniel KomisarekGND, Carsten SchauerteGND, Klaus MerzGND |
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URN: | urn:nbn:de:hbz:294-78044 |
DOI: | https://doi.org/10.3390/chemistry2010009 |
Parent Title (English): | Chemistry |
Publisher: | MDPI |
Place of publication: | Basel |
Document Type: | Article |
Language: | English |
Date of Publication (online): | 2021/01/27 |
Date of first Publication: | 2020/03/04 |
Publishing Institution: | Ruhr-Universität Bochum, Universitätsbibliothek |
Tag: | Open Access Fonds cocrystal synthesis; cocrystallization mechanism; multicomponent cocrystal |
Volume: | 2 |
Issue: | 1 |
First Page: | 93 |
Last Page: | 100 |
Note: | Article Processing Charge funded by the Deutsche Forschungsgemeinschaft (DFG) and the Open Access Publication Fund of Ruhr-Universität Bochum. |
Institutes/Facilities: | Lehrstuhl für anorganische Chemie |
Dewey Decimal Classification: | Naturwissenschaften und Mathematik / Chemie, Kristallographie, Mineralogie |
open_access (DINI-Set): | open_access |
Licence (English): | Creative Commons - CC BY 4.0 - Attribution 4.0 International |